Mechanochemical Bromination of Naphthalene Catalyzed by Zeolites: From Small Scale to Continuous Synthesis
نویسندگان
چکیده
Catalyzed reactions of organic substrates that operate continuously by extrusion techniques are rare. In this study, we developed a mechanochemical bromination unactivated naphthalene (1) with 1,3-dibromo-5,5-dimethylhydantoin (DBDMH), catalyzed zeolites in ball mill. The use DBDMH enabled the atom economy reaction to be superior compared other brominating agents evaluated. Among tested, FAU-type zeolite demonstrated high catalytic activity and recyclability. success route on small scale development continuous 1 twin-screw extrusion.
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ژورنال
عنوان ژورنال: Chemistry methods
سال: 2022
ISSN: ['2628-9725']
DOI: https://doi.org/10.1002/cmtd.202200035